本书内容主要涉及聚合物的形态结构、高分子溶液的性质、聚合物的力学性能、聚合物的热性能、聚合物的加工性能、聚合物的电性能以及聚合物乳液的性质等方面，共精选了20个实验，都是合成与加工中需要做的一些测试方法和手段。每个实验都介绍与实验有关的基本原理和明确的目的要求、实验步骤、仪器和药品、数据处理以及需要思考的问题等；书后附有12个附表，方便查阅。本书充分体现了重庆文理学院高分子物理实验教学的特色，体现了作者近年的教学研究成果与科研成果。
目 录
单元 聚合物的溶液性质································································································ 1
实验一 聚合物的逐步沉淀分级法··················································································· 1
实验二 黏度法测定聚合物分子量··················································································· 6
实验三 聚合物的溶解································································································· 10
实验四 聚合物表面的接触角测定················································································· 14
二单元 聚合物的结构分析······························································································· 17
实验五 溶胀平衡法测定聚合物的交联度······································································· 17
实验六 偏光显微镜法观察聚合物球晶··········································································· 22
实验七 结晶速率仪测定聚合物的结晶速率···································································· 25
实验八 红外光谱法鉴定聚合物···················································································· 29
实验九 偏光显微镜法观察聚合物球晶形态···································································· 32
三单元 聚合物的热性能·································································································· 38
实验十 转矩流变仪测聚氯乙烯热稳定性······································································· 38
实验十一 差示扫描量热法（DSC）测定聚合物的热性能················································· 43
实验十二 热重法（TG）测定聚合物热降解反应动力学参数············································ 47
实验十三 聚合物耐热性能的测试················································································· 54
四单元 聚合物的力学性能······························································································· 58
实验十四 聚合物冲击性能的测试················································································· 58
实验十五 聚合物拉伸性能的测试················································································· 62
实验十六 聚合物硬度的测试························································································ 65
五单元 聚合物的加工性能······························································································· 68
实验十七 热塑性塑料聚氯乙烯的塑化、力学性能试样压制、成型实验····························· 68
实验十八 热塑性塑料的挤出造粒与注塑成型································································· 73
六单元 聚合物熔体的其他性质（熔体流动特性、电性能）················································· 83
实验十九 高聚物熔体流动特性的测试··········································································· 83
实验二十 高阻仪测定聚合物的电阻·············································································· 87
附 表······························································································································· 94
主要参考文献··················································································································· 105
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